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After aligning and suspending the fibersover the walls, the samples are pyrolyzed at 900°C in an inert N2environment. Fibers were successfully aligned on the Carbon-MEMS substrates, as shown in Figure 5. The operating voltage in LVNFES can be lowered down to 100V without any interruption of the electrospinning jet and has a strong influence on fiber thickness (also established in our previous report on LVNFES  and as seen in Figure 5). Lowering the operating voltage enables thinner fibers to be deposited.
911. –Wien:Springer-Verlag,1953. In book“Research and application of rhenium alloys”. Moscow. Publisher “Science”. 1975. 54-56. 140-157. 2010. 28-37. Technology of mechanical engineering. 2010. 17-22. Article 08JG04. Procedia CIRP 1(2012)318–323. 628-637. edu Keywords: Electrospinning, Carbon nanofibers, Low voltage near-field electrospinning, Oxygen plasma Abstract. A multitude of applications can take advantage of these patterned carbon nanofibers especially in the field of electrochemical sensors and nanoelectronics.
Figure1. SEM image of Ag2Se nanowires (inset is SEM image of Ag2Se nanowire at high magnification). Figure 2. EDAX Spectrum of Ag2Se nanowires. Fig. 3 shows the XRD spectrum of as-deposited β-Ag2Se nanowires. The diffraction peaks at different values of 2θ along with their d-values and miller indices (hkl) are shown in table 1, which confirm orthorhombic crystal structure of Ag2Se . It is in well agreement with that of polycrystalline bulk Ag2Se standard. Similar diffraction peaks of Ag2Se were observed and reported by Chen et al and Gates et al [ 25].